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Astrid Campos-Mata

Publications and source records attributed to Astrid Campos-Mata.

2 recordsLinked to original sources

Facet- and thickness-dependent band-edge alignment at ZrSe\texorpdfstring{$_3$}{3} surfaces: hybrid-functional calculations with spin-orbit coupling

Transition-metal trichalcogenides MX$_3$ are quasi-one-dimensional van der Waals materials whose layers form through lateral chain binding, giving them an interlayer cleavage plane and in-plane electronic anisotropy. Among them, ZrSe$_3$ is stable under ambient conditions and semiconducting. Exfoliated crystals expose four crystallographic planes, and electrocatalytic measurements on an individual crystal assigned the hydrogen evolution activity to the high-energy (210) facet rather than to the basal plane. Those non-basal surfaces remain uncharacterized, since the available calculations treat either the bulk crystal or the free-standing basal monolayer. Here, we compute the surface energies and the equilibrium morphology of these four surfaces with a dispersion-corrected semilocal functional, and their band-edge alignment with the HSE06 hybrid functional including spin-orbit coupling. The surface energies span nearly an order of magnitude, from \SI{0.097}{\joule\per\meter\squared} for (001) to \SI{0.869}{\joule\per\meter\squared} for (010), and the Wulff shape exposes the four observed planes with area fractions of \SI{17.1}{\percent}, \SI{4.4}{\percent}, \SI{71.4}{\percent}, and \SI{7.0}{\percent}. The ionization potential varies by \SI{0.45}{\electronvolt} between facets and the electron affinity by \SI{0.80}{\electronvolt}, the gap of (210) falls from 1.43 to \SI{0.94}{\electronvolt} between 10 and \SI{23}{\angstrom}, and (010) remains metallic. The facets separate according to whether the cut preserves or distorts the Se-Se dimer, and the distorted dimers concentrate the frontier states. Because the same dimer governs the bulk electronic structure of the MX$_3$ family, the criterion transfers to the related trichalcogenides.

cond-mat.mtrl-sci↗

Structure-Property Correlation of Cr/Cu-MnFeCoNi High-Entropy Alloys for Alkaline Water Electrolysis

High-entropy alloys (HEAs), with their unique compositional-complexity and tunable surface chemistry, have emerged as promising electrocatalysts for energy conversion. The catalytic activity of HEA often arises from the interplay between the intrinsic activity of the individual elements and the synergistic effects generated at the interfaces. Even a single-element substitution in a multicomponent HEA can substantially alter the surface-chemistry and electrochemical kinetics of the active surface. Here we investigated the structure-property relationship of CrMnFeCoNi (HEA-Cr) and MnFeCoNiCu (HEA-Cu) HEAs by comparing the alkaline hydrogen evolution reaction (HER) and oxygen evolution reaction (OER) activity. Under the same experimental condition, HEA-Cu outperforms HEA-Cr towards both HER and OER. Substituting Cr with Cu significantly enhances the bifunctional activity, where HEA-Cu achieved a lower overpotential (538 mV) and Tafel slope (165 mVdec-1) when compared with HEA-Cr. Computational analysis corroborates these findings, showing that Cu substitution modulates the electronic-structure to provide favorable binding energies for reaction intermediates (H*, O*, OH*, and OOH*). Interestingly, unlike HER, recovered HEA-Cu after OER showed migration of Cu forming a Cu-rich outer layer shell with a multimetallic core. These findings demonstrate the potential of single-element substitution in HEAs as a strategy for designing high-performance, cost-effective catalysts for efficient water electrolysis.

cond-mat.mtrl-sci↗